FreeZone Triad Benchtop Freeze Dryer on FreeZone Cart with Scroll Pump with Model

FreeZone Triad -84 C, -121 F Freeze Dryers

FreeZone Triad Benchtop Freeze Dryers are designed for multiple types of lyophilization: flask, bulk and stoppering vials. With the ability to freeze dry samples in so many different forms, the Triad's versatility and compact design make it perfect for busy labs.

The upright stainless steel collector coil holds 2.5 liters of ice before defrosting. Two 1/3 hp HCFC/CFC-free refrigeration compressors cool the collector to -84° C (-121° F), suitable for aqueous or dilute acetonitrile samples. Temperature-controlled shelves range from -55° C to +50° C (-67° F to +122° F) and a maximum of -75° C (-103° F) during pre-freezing. The shelves provide pneumatic stoppering with a diaphragm, eliminating the need for compressed gas.

Lyo-Works™ OS provides a real time display of collector temperature and vacuum level, shown on a 5" full color, capacitive touchscreen. A stoppering tray dryer and four valve ports are built-in.

Vacuum pump and freeze dry glassware (if not bulk freeze drying) are required (not included).

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These all-in-one, dual refrigeration freeze dryers/stoppering tray dryers reach -84° C for processing low eutectic point samples. One large shelf holds small containers or bulk samples.

Features (All Models)

Stainless steel collector coil capable of removing 1.84 L of water in 24 hours and holding 2.5 L of ice before defrosting
Two 1/3 hp HCFC/CFC-free refrigeration compressors cool the collector to -84° C (-121° F) and work in concert with a 1000-watt heater to cool and heat fluid medium circulating through channels in the shelf. Not for use with samples containing methanol or ethanol
Processing shelf, 12.4" w x 14.5" d (31.5 x 36.8 cm). Spacing between shelf and top of chamber accommodates containers with stoppers up to 148 mm maximum height
One probe for monitoring temperature of sample in chamber
Temperature ramp and hold programming from -55° C to +50° C (-67° F to +122° F) and -75° C (-103° F) during pre-freezing. Controls temperature to ±1° C of set point. Memory to store 30 programs with 16 segments each including number of steps, ramp rate, shelf temperature, hold time and vacuum level
Full color, 5" capacitive touchscreen with Lyo-Works™ OS:
- Real time display of collector temperature and vacuum level
- Creation and storage for up to 30 programs with up to 16 steps each. Ability to set ramp rate, shelf temperature, shelf temperature time and vacuum set point per step
- Manual start-up buttons for collector and shelf temperature control and vacuum pull down
- Alerts, diagnostic tests, user manual and defrost control
- Data logging stores and displays data in table or graph format, and may be exported via USB or Ethernet
- Settings include language (English, Spanish, German, French, Italian, Chinese, Japanese, Portuguese), time, temperature (° C or ° F) and vacuum (mBar, Torr or Pa)
- Alerts can be emailed to user-entered addresses via Ethernet connection
- Vacuum pump maintenance alert
- Security lock-out
Pneumatic stoppering mechanism with diaphragm and plate. No compressed gas is required
Stoppering control knob, vacuum release control knob and 1/8" OD user-supplied sterile/inert gas backfill port
Four left side-mounted neoprene valves with molded plastic knobs and fittings that accommodate 1/2" and 3/4" flask adapters
USB port and Ethernet connection
Electrical receptacle for vacuum pump
Hot gas defrost with stainless steel drain pan, silicone drain hose and auto shut off at +60° C (+140° F)
Vacuum control valve
Vacuum break valve
Stainless steel and powder-coated steel exterior
Clear acrylic door, 1" thick, with silicone gasket and latch 3/4" OD vacuum connection. 36" long, 3/4" ID vacuum hose with two clamps

Options Include

Region-specific electrical plug configurations

Required Accessories (Not Included)

Vacuum pump with a displacement of at least 98 L/min, 0.002 mBar ultimate pressure and fitting for 3/4" ID vacuum hose

Our Product Representatives Are Here To Help

Labconco's FreeZone Triad Freeze Dryer

This video demonstrates how the FreeZone Triad Benchtop Freeze Dryer is designed to lyophilize the widest variety of sample types: from bulk items, vials and microplates on heated shelves to large samples in flasks.

Gail's Story Changed the Way We Think About Lab Freeze Drying

When she visited Kelly at Labconco, Gail's struggle led to an epiphany that would change how laboratory freeze drying is done. With the creation of Lyo-Works OS, samples can now be monitored from anywhere. And with End-Zone™ End Point Detection, now FreeZone Freeze Dryers can even send you an alert when your samples are completely lyophilized.

End-Zone End Point Detection System-Set Up

Know as soon as your samples reach dryness. Set up your End-Zone™ End Point Detection System to alert you when the primary drying phase is complete for up to 5 samples in 600ml or larger flasks. This video shows how to install and operate the system.

Programming the FreeZone Triad

Instructions for programming your FreeZone Triad Freeze Dryer.

Troubleshooting Vacuum Leaks in Labconco Lyophilizers

Learn to troublesoot vacuum leaks in Labconco FreeZone Freeze Dry Systems

Preparing Pre-freeze Samples in Flasks for Lyophilization

Here are some simple tips to get the best results when freeze drying. These tips can also help you avoid breaking glassware, and help you select the best method of freeze dry preparation.

Literature & Resources

Brochures
- FreeZone Freeze Dryers Catalog
  Contains a selection guide, features and benefits, specifications and ordering information on the complete line of FreeZone Freeze Dry Systems, with collector capacities from 2.5 to 18 liters; FreeZone Triad Freeze Dryers; FreeZone Stoppering Tray Dryers; FreeZone Bulk Tray Dryers; drying accessories; glassware and vacuum pumps.
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- French-Language FreeZone Freeze Dryers Catalog
  This French-language catalog contains an overview, features, benefits, specifications and ordering information on FreeZone Freeze Dryers. Ordering information on accessories is also included. En français.
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User's Manuals
- FreeZone Triad Freeze Dryers Manual
  For catalog numbers in the 7940010xx series. These are FreeZone Triad Benchtop Freeze Dryers with Lyo-Works™ OS manufactured in September 2018 or later.
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- Freeze Dry Chemical Compatibility/Eutectic Temperature Chart
  This chart provides common chemicals, their eutectic temperatures, recommended collector temperature, liquid nitrogen trap recommendation and rotary vane pump recommendation as they relate to FreeZone Freeze Dry Systems.
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- Freeze Dry Vacuum System Troubleshooting
  Provides instructions and illustrations to help solve vacuum leaks.
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- FreeZone Triad Freeze Dry System Manual (French)
  Mode d'emploi: Lyophilisatuer pilote: FreeZone TriadFor catalog numbers: 7400030 and 7400040
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Application Notes
- Methodologies using the Freeze Dryer
  Approximate Freeze Drying Times, Procedure for Freeze Drying Fish Samples for Volatile Substances Using a 4.5 Liter Freeze Dry System, Extraction and Analytical Method for "Microcystin LR" in Cyanobacteria Samples, General Freeze Dry Application for Snake Venom and Other Small Volume Samples of 0.4 ml or Less, Freeze Drying Fungi, General Freeze Dry Application for Monitoring Soil Samples, Freeze Dry Applications for Monitoring Anti-Cancer Drugs and Freeze Drying Mango Powder.
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Safety Data Sheets
- Lexsol 542 SDS
  Safety data sheet for heat transfer solution used in FreeZone Stoppering Tray Dryers manufactured since 2004 and FreeZone Triad Freeze Dry Systems.
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- Pentane MSDS
  This is a material safety data sheet for Pentane refrigerant, which is used in FreeZone Plus (-84) Cascade Freeze Dry Systems, FreeZone Triad Freeze Dry Systems and CentriVap -84 Cold Traps.
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- Refrigerant Genetron AZ-50 (R507) MSDS
  Material safety data sheet for refrigerant used in FreeZone 1, 2.5, 4.5, 6, 12, 18 Liter Freeze Dry Systems, FreeZone Plus 2.5, 6 and 12 Liter Cascade Freeze Dry Systems, FreeZone Triad Freeze Dry Systems, FreeZone Stoppering Tray Dryers, CentriVap Mobile Systems, Refrigerated CentriVap Vacuum Concentrators and CentriVap Ultra-Low Cold Traps.
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- Refrigerant R452A SDS
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- Refrigerant R508B MSDS
  Material safety data sheet for refrigerant used in FreeZone Plus 2.5, 4.5, 6 and 12 Liter Cascade Freeze Dry Systems, FreeZone Triad Freeze Dry Systems and CentriVap Ultra-Low Cold Traps.
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Installation Qualification / Operation Qualification
- Installation Qualification/Operation Qualification for FreeZone Triad Freeze Dryers
  For validation of predetermined FreeZone Triad Freeze Dryers specifications. Provides a checklist of installation and operation qualifications to complete when beginning operation on new or used FreeZone Triad Freeze Dryers manufactured in September 2018 or later. These systems have Lyo-Works™ OS, blue control panel labels and stainless steel fronts.
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Software & Apps
- Lyo-Works OS Software for FreeZone Triad
  This is the Lyo-Works application software for your FreeZone Triad's touchscreen Android interface. The .zip file includes installation instructions. Extract the files in order to install.
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